Xiangyun Gao (1), Bao Lei (2), Yi Zhang (1), Daxu Zhang (3), Chong Wei (1), Laifei Cheng (1), Litong Zhang (1), Xugin Li (4), Hao Ding (5)
Materials Characterization. Volume 196 (February 2023). DOI: https://doi.org/10.1016/j.matchar.2022.112608

Keywords

Ceramic matrix composite (CMC), microstructure, computed tomography (CT), image segmentation, deep learning

Abstract

Continuous silicon carbide fibre reinforced silicon carbide ceramic matrix composite(SiC/SiC) is a multiphase non-homogeneous anisotropic material used in new generation aero-engines. However, it is difficult to identify its microstructural features and related complex spatial distributions, which determine its mechanical properties. Herein, shallow cross-linked (2.5D) SiC/SiC, fibre bundle SiC/SiC and filament SiC/SiC were prepared by chemical vapor infiltration and their tensile properties were tested. Microstructural features and damage characteristics were studied using micro and nano computed tomography (CT). Deep learning was applied to process the CT images to obtain complex 3D structural features of the composite, especially with the help of segmentation using ORS Dragonfly software. Structural units such as fibre, interphase and matrix, as well as damage features such as matrix cracks, pull-out holes and pull-out fibres were accurately identified at macro-scale, meso-scale and micro-scale (2.5D architecture, bundle and filament, respectively). Important characteristics such as porosity, fibre pull-out length distribution and periodic crack distribution were obtained. This information would be helpful to understand the macro/microscopic mechanical behaviours of SiC/SiC composites and optimize their preparation process.

How Our Software Was Used

Ceramic matrix composite was segmented using a deep learning model trained in Dragonfly.

Author Affiliation

(1) Science and Technology on Thermostructural Composite Materials Laboratory, Northwestern Polytechnical University, Xi'an, Shaanxi 710072, PR China
(2) China Academy of Launch Vehicle Technology, Beijing 100076, PR China
(3) School of Naval Architecture, Ocean & Civil Engineering, Shanghai Jiao Tong University, Shanghai 200240, PR China
(4) School of Materials and Environmental Engineering, Chengdu Technological University, Chengdu 611730, PR China
(5) School of Materials Science and Engineering, Harbin Institute of Technology, Harbin 150001, PR China